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[Data] Sublimation Purification Device for Organic Materials

Published information on 'Sublimation purification of organic semiconductor materials' and 'Principles of sublimation purification'!

This document introduces sublimation purification equipment for organic materials. It includes sections on "Sublimation Purification of Organic Semiconductor Materials," "Principles of Sublimation Purification," and "Practical Aspects of Sublimation Purification." Additionally, it explains the "Configuration of Sublimation Purification Equipment" and "Sample Recovery Tube After Sublimation Purification" with accompanying diagrams. [Contents] ■ Sublimation Purification of Organic Semiconductor Materials ■ Principles of Sublimation Purification ■ Practical Aspects of Sublimation Purification *For more details, please refer to the PDF document or feel free to contact us.

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Sublimation Refinement Device P-100 Series

It is possible to purify in units of several grams using the sublimation purification device.

Our company manufactures and sells the "Sublimation Purification Device P-100 Series," which is capable of purification in the range of several grams. 【Features】 ○ Suitable size for small-scale purification with input amounts of around several grams ○ Easy structure for sample loading and unloading ○ Capable of heating up to 450°C, making it applicable to most materials ○ Equipped with four thermocouples outside the heater section, allowing for optimal determination of the re-crystallization position ○ Ability to confirm the purification state ○ Uses Pfeiffer turbo molecular pump and membrane pump in the exhaust system, enabling easy attainment of a clean vacuum through a completely dry exhaust system ○ Equipped with a large-sized liquid nitrogen trap ○ Easy maintenance structure ○ Equipped with a full-range vacuum gauge capable of continuous measurement from atmospheric pressure to high vacuum ○ Can be connected to a glove box (custom specification) ○ Space-saving design ensuring high performance

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-What is sublimation refining- Evolution of sublimation refining equipment through advanced technology *Video available

- Sublimation refinement - Everything started with the redefinition of sublimation refinement - The QUANTIpure -

- Sublimation - This term refers to the phenomenon where a substance transitions directly from the solid phase to the gas phase without passing through the liquid phase. Conversely, it also refers to the phenomenon of transitioning from the gas phase to the solid phase, but these are generally referred to as deposition, solidification, or recrystallization. - Conditions for the Occurrence of Sublimation - Common substances exhibit three states: solid, liquid, and gas, which are determined by temperature changes. The boundary temperatures are defined by the "vapor pressure" of each substance. Since the phase change temperature is dictated by vapor pressure, by altering the environmental conditions (reducing pressure), sublimation can occur in many substances without passing through the liquid phase. - Applications of Sublimation and Sublimation Purification Devices - Many compounds have their own specific sublimation and solidification temperatures. By utilizing this temperature difference, it is possible to significantly separate mixed compounds. This phenomenon is applied in sublimation purification devices. Taking advantage of the property that allows direct phase transition from solid to gas, it is widely used for the high purification of "insoluble" substances that are difficult to dissolve in solvents.

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  • Organic EL

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